Experimental Design
n
A lifetime studywas performed by repetitively
injecting a standardmixture designed forASTM
D2887 calibration.
n
APolywax 1000 samplewas injected and
resolution betweenC50 andC52was calculated
according to themethod.
n
Record kept of the retention time for C52 and the
bleed at 430
l
o
o
C over the course of the experiment.
n
Repeated until the column resolution fell below
ASTMD6352-98 specifications.
