GC
Agilent 6890
InjectionPort Temperature: 250°C
Carrier gas:
helium, constant flow
Flow rate:
2.3ml/min, 25.6psi@40°C.
Oven temperature:
40°C (hold2min.) to55°C@4°C/min. (nohold)
to 110°C@
25°C/min.
(hold2min.) to250°C@
25°C/min (hold5minutes)
Total Runtime:
20.55minutes
Agilent Dual Flame IonizationDetectors
Restek’sStop-FlowUnit PulseSettings:
InjectionPort Connection:
cool-on-column injector.
Pressure:
31.0PSI constant pressure
Pulses:
ValveClosed 0.00minutes.
ValveOpen
3.00minutes
ValveClosed 3.15minutes
ValveOpen 4.65minutes
ValveClosed 5.02minutes
ValveOpen 5.10minutes
ValveClosed 5.40minutes
