Residual Solvents: RunConditions
Dual FIDs@ 250°C
Dual FIDs@ 250°C
Detectors
0.2
µ
LHS, 200:1split
0.2
µ
LHS, 200:1split
Injection
230°C
230°C
Injector
2.5mL/min. to9.5min.
3.5mL/min. at 10min.
1.5mL/min.
constant flow
ColumnFlow
40°C (1min. hold)
to 65°C at 6°C/min.,
to100°Cat 12°C/min.,
to250°Cat 70°C/min.,
1.8min. hold
40°C (6min. hold)
to100°Cat 4°C/min.,
to220°Cat 15°C/min.,
5min. hold
OvenProgram
Stabilwax
15mx0.25mm, 0.5
µ
m
Rtx-200
30mx0.25mm, 1
µ
m
Stabilwax
15mx0.25mm, 0.5
µ
m
Rtx-200
30mx0.25mm, 1
µ
m
Analytical
Columns
Fast Procedure
StandardProcedure
