Table I. GCprogram for the volatile compounds analyzed inFigure3.
Columns:
Rtx®-VMS, 10m x 0.18mm x 1.0
µ
m
Stabilwax
®
-DA, 10m x 0.18mm x 0.18
µ
m
Injector:
250°C, 1
µ
L split injection (150:1)
CarrierGas:
hydrogenat 25psi, constant pressure
Oven:
35°C (0.5min. hold)
to45°Cat 20°C/min.
to210°Cat 100°C/min. (1-4min. hold)
Detector:
FID@250°C
Air@400cc/min.
H2@40cc/min.
N2@40cc/min.
