USP<467>Common solvents
Method I:
G2730mx 0.53mmx 5.0µmdf, w/5mPMguard
Inj:
Headspace at 500ppmin bulkpharm. 2:1 split
OvenTemp
: 35(10)5/100 (0) 25/240(5)
Detector:
FID, 260°C, 1 x10
-11
AFS
Carrier:
helium, 4.1psi const., 35cm/sec@35°C
Samples shaken andheated at 90°Cfor 15minutes, 1mL
headspace injection.
