USP<467>Method IV
Method IV:
G43 30mx 0.53mmx 3.0µmdf
Inj:
100µLcat#36007 in 5mLwater, 1g sodiumsulphate in
20mLheadspace vial
OvenTemp
: 40(20)35/240(20)
Detector:
FID, 260°C, 1.25 x10
-11
AFS
Carrier:
helium, 3.5psi const., 35cm/sec@40°C
SplitRatio:
2:1
Concentrator:
ThermoQuest HS2000Headspace
AutosamplerVial 80°C, 60min. shaker on
