Organophosphorus Pesticides:
MSData
GCoven: 80°C (0.5min) up12°C/min to
280°C (15min)
Injector:
200°Csplitless, hold time1min,
4mmsinglegooseneck Siltek sleeve
Detector: Agilent 5971AMSD
full scan50-550AMU
DT@80°C=1.44min, heliumcarrier
Column:
RTX-OPPesticides2, cat# 11241
30mx0.32mmID, 0.32µm
9
12
15
18
21
