ChlorinatedPesticides
Analytical conditions
GCoven: 120°C(1min) upat 20°C /min to245°C,
up at 6°C /min to 310°C
Injector: 220°C, splitless, 1minpurgeoff hold,
4mmsinglegooseneck Siltek sleeve
Detector: 310°C, Agilent ECD
Column:
Stx-CLPesticides onSiltek, cat#11544
30mx0.32mmID, 0.5µm
Rtx-CLPesticides, cat# 11139
30mx0.32mmID, 0.5µm
Column:
Stx-CLPesticides 2 onSiltek, cat#11444
30mx0.32ID, 0.25µm
Rtx-CLPesticides 2, cat#11324
30mx0.32mmID, 0.25µm
RT# Analyte
1 2,4,5,6 tetrachloro-m-xylene - surrogate
2 alpha-BHC
3 gamma-BHC
4 beta-BHC
5 delta-BHC
6 heptachlor
7 aldrin
8 heptachlor epoxide
9 gamma-chlordane
10 alpha-chlordane
11 4,4'
DDE
12 endosulfan I
13 dieldrin
14 endrin
15 4,4'
DDD
16 endosulfan II
17 4,4'
DDT
18 endrin aldehyde
19 methoxychlor
20 endosulfan sulfate
21 endrin ketone
22 decachlorobiphenyl - surrogate
