restekadv07 - page 166

with data pack with data pack
• 9 • www.restekcorp.com 800-356-1688
NewAnalytical Reference
Materials
FAMEs, Acetates, BTEX, Glycols
n-amyl acetate
butyl acetate
ethyl acetate
isopropyl acetate
methyl acetate
propyl acetate
vinyl acetate
8260BAcetateMix (7 components)
• Includesmethyl acetate and n-amyl acetate.
benzene
ethylbenzene
toluene
m-xylene*
o-xylene
p-xylene*
2,000µg/mL each in P&Tmethanol, 1mL/ampul
BTEX Standard (6 components)
• m- and p-xylene at 1/2 concentration.
• Contact Restek for future formulations.
Each 5-pk. 10-pk.
30488 30488-510
w/data pack 30488-500 30488-520 30588
Each 5-pk. 10-pk.
30489 30489-510
w/data pack 30489-500 30489-520 30589
ethylene glycol propylene glycol
50,000µg/mL each inDI water, 1mL/ampul
Glycols Standard
Each 5-pk. 10-pk.
30471 30471-510
w/data pack 30471-500 30471-520 30571
Ordering Information | Rtx ®-5SilMSColumns (FusedSilica)
(Equivalent selectivity of Crossbond® 5% diphenyl/95% dimethyl polysiloxane) Stable to 360°C
ID df (µm) temp. limits 15-Meter 30-Meter
0.25mm 0.10 -60 to 330/350°C 12705 12708
0.25 -60 to 330/350°C 12720 12723
0.50 -60 to 330/350°C 12735 12738
1.00 -60 to 325/350°C 12750 12753
GC_EV00629
1. N-nitrosodimethylamine
2. pyridine
3. 2-fluorophenol
4. phenol-d6
5. phenol
6. aniline
7. bis(2-chloroethyl)ether
8. 2-chlorophenol
9. 1,3-dichlorobenzene
10. 1,4-dichlorobenzene-d4
11. 1,4-dichlorobenzene
12. benzyl alcohol
13. 1,2-dichlorobenzene
14. 2-methylphenol
15. bis(2-chloroisopropyl)ether
16. 4-methylphenol/
3-methylphenol*
17. N-nitroso-di-n-
propylamine
18. hexachloroethane
19. nitrobenzene-d5
20. nitrobenzene
21. isophorone
22. 2-nitrophenol
23. 2,4-dimethylphenol
24. bis(2-chloroethoxy)methane
25. benzoic acid
26. 2,4-dichlorophenol
27. 1,2,4-trichlorobenzene
28. naphthalene-d8
29. naphthalene
30. 4-chloroanaline
31. hexachlorobutadiene
32. 4-chloro-3-methylphenol
33. 2-methylnaphthalene
34. 1-methylnaphthalene
35. hexachlorocyclopenta-
diene
36. 2,4,6-trichlorophenol
37. 2,4,5-trichlorophenol
38. 2-fluorobiphenyl
39. 2-chloronaphthalene
40. 2-nitroaniline
41. 1,4-dinitrobenzene
42. dimethylphthalate
43. 1,3-dinitrobenzene
44. 2,6-dinitrotoluene
45. acenaphthylene
46. 1,2-dinitrobenzene
47. 3-nitroaniline
48. acenaphthene-d10
49. acenaphthene
50. 2,4-dinitrophenol
51. 4-nitrophenol
52. dibenzofuran
53. 2,4-dinitrotoluene
54. 2,3,4,6-tetrachlorophenol
55. 2,3,5,6-tetrachlorophenol
56. diethyl phthalate
57. 4-chlorophenyl phenyl
ether
58. fluorene
59. 4-nitroaniline
60. 4,6-dinitro-2-methylphenol
61. diphenylamine**
62. azobenzene***
63. 2,4,6-tribromophenol
64. 4-bromophenyl phenyl
ether
65. hexachlorobenzene
66. pentachlorophenol
67. phenanthrene-d10
68. phenanthrene
69. anthracene
70. carbazole
71. di- n-butylphthalate
72. fluoranthene
73. benzidine
74. pyrene
75. p-terphenyl-d14
76. butyl benzyl phthalate
77. bis(2-ethylhexyl)adipate
78. benzo(a)anthracene
79. chrysene-d12
80. chrysene
81. bis(2-ethylhexyl)phthalate
82. di- n-octyl phthalate
83. benzo(b)fluoranthene
84. benzo(k)fluoranthene
85. benzo(a)pyrene
86. perylene-d12
87. indeno(1,2,3-cd)pyrene
88. dibenzo(a,h)anthracene
89. benzo(ghi)perylene
*Each at 0.5x concentration of other components.
**N-nitrosodiphenylamine (8270-listed analyte) decomposes
to diphenylamine (mix component).
***1,2-diphenylhydrazine (8270-listed analyte) decomposes to
azobenzene (mix component).
Column: Rtx®-5Sil MSw/ 5-meter Integra-Guard™
30m, 0.25mm ID, 0.25µm
(cat.# 12723-124)
Instrument: Agilent 5973GC/MS
Sample: US EPAMethod 8270DMix 1µL,
16 ppm each component (16ng on column)
8270MegaMix™ (cat.# 31686)
Benzoic Acid Standard (cat.# 31415)
Benzidine Standard (cat.# 31441)
Acid SurrogateMix (4/89 SOW)(cat.# 31063)
B/NSurrogate StandardMix
(4/89 SOW) (cat.# 31062)
SV Internal StandardMix (cat.# 31006)
Solvent: dichloromethane
Inj.: 1.0µL splitless (hold 0.3min.),
4mmDrilledUniliner® (cat.# 21055)
Inj. temp.: 300°C
Carrier gas: helium, constant flow
Flow rate: 1.1mL/min.
Dead Time: 1.8minutes@ 35°C
Oven temp.: 35°C (hold 4min.) to 245°C@
25°C/min. (no hold) to 330°C@
6°C/min.(hold 3min.)
Det: GC/MS
Transfer line temp.: 280°C
Scan range: 35–550 amu
Solvent Delay: 5min.
Tune: DFTPP
Ionization: EI
Bold indicates a component
of the 8270DMegaMix™
1,000µg/mL each (except noted) inmethylene chloride:ben-
zene (75:25), 1mL/ampul
8270MegaMix ™ (76 components)
Each 5-pk. 10-pk.
31686 31686-510 —
31686-500 31686-520 31786
8270Matrix SpikeMix (76 components)
Each 5-pk. 10-pk.
31687 31687-510 —
31687-500 31687-520 31787
200µg/mL each (except noted) inmethanol:methylene
chloride:benzene (80:15:5), 5mL/ampul
See bold compounds in Figure 1 peak list. See bold compounds in Figure 1 peak list.
Chain % byWeight
C4:0 4.0
C6:0 4.0
C8:0 4.0
C10:0 4.0
C11:0 2.0
C12:0 4.0
C13: 2.0
C14:0 4.0
C14:1( cis-9) 2.0
C15:0 2.0
C15:1( cis-10) 2.0
C16:0 6.0
C16;1( cis-9) 2.0
C17:0 2.0
C17:1( cis-10) 2.0
C18:0 4.0
C18:1( trans-9) 2.0
C18:1( cis-9) 4.0
C18:2(all- trans-9.12) 2.0
C18:2(all- cis-9,12) 2.0
C18:3(all- cis6,9,12) 2.0
C18:3(all- cis9,12,15) 2.0
C20:0 4.0
C20:1( cis-11) 2.0
C20:2(all- cis11,14) 2.0
C20:3 (all- cis8,11,14) 2.0
C20:3(all- cis11,14,17) 2.0
C20:4(all- cis5,8,11,14) 2.0
C20:5(all- cis5,8,11,14,17) 2.0
C21:0 2.0
C22:0 4.0
C22:1( cis13) 2.0
C22:2(all- cis13,16) 2.0
22:6(all- cis4,7,10,13,16,19) 2.0
C23:0 2.0
C24:0 4.0
C24:1( cis-15) 2.0
30mg/mL inmethylene chloride, 1mL/ampul
Food Industry FAMEMix
(37 components)
ea.
35077
2,000µg/mL each in P&Tmethanol, 1mL/ampul
*1,000µg/mL
• Assay for de-icing compounds.
• Includes trans FAMEs.