555
GCCHROMATOGRAMS |
ENVIRONMENTAL
Semivolatiles
Column:
Rtx
®
-5Sil MS, 30m, 0.25mm ID, 0.25µm (cat.# 12723)
Sample:
50µg/mL 610 PAHMix (cat.# 31011)
inmethylene chloride
Inj.:
1.0µL splitless (hold 2min.),
2mm splitless inlet liner w/wool (cat.# 20829)
Inj. temp.:
330°C
Carrier gas:
hydrogen, 4mL/min. constant flow
Oven temp.:
40°C (hold 2min.) to 250°C@ 25°C/min. to 265°C@ 5°C/min.
to 300°C (hold 4min.)@ 25°C/min.
Det.:
FID@ 350°C
1. naphthalene
2. acenaphthylene
3. acenaphthene
4. fluorene
5. phenanthrene
6. anthracene
7. fluoranthene
8. pyrene
9. benzo(a)anthracene
10. chrysene
11. benzo(b)fluoranthene
12. benzo(k)fluoranthene
13. benzo(a)pyrene
14. indeno(1,2,3-cd)pyrene
15. dibenzo(a,h)anthracene
16. benzo(ghi)perylene
GC_EV00595
PolycyclicAromaticHydrocarbons
USEPAMethod610
Rtx®-5SilMS
PAHs resolved in
less than16min.!
1.0
2.0
3.0
4.0
5.0
6.0
7.0
8.0
9.0
10. 0
1. naphthalene
2. acenaphthylene
3. acenaphthene
4. fluorene
5. phenanthrene
6. anthracene
7. fluoranthene
8. pyrene
9. benzo(a)anthracene
10. chrysene
11. benzo(b)fluoranthene
12. benzo(k)fluoranthene
13. benzo(a)pyrene
14. indeno(1,2,3-cd)pyrene
15. dibenzo(a,h)anthracene
16. benzo(ghi)perylene
PolycyclicAromaticHydrocarbons
USEPAMethod610
Rxi®-5SilMS (20mx0.18mmx0.18μm)
Column:
Rxi
®
-5Sil MS, 20m, 0.18mm ID, 0.18µm (cat.# 43602)
Sample:
610 PAHMix, 10ppm (cat.# 31011)
Instrument:
PerkinElmer Clarus 600
Inj.:
0.5µL splitless (hold 1.75min.), 2mm split/splitless liner w/wool (cat.# 21718)
Inj. temp.:
320°C
Carrier gas:
helium, constant flow
Linear velocity: 37cm/sec.@ 45°C
Oven temp.:
45°C (hold 0.5min.) to 150°C@ 95°C/min. to 270°C@ 45°C/min. to 300°C@ 7°C/min.
Det.:
FID@ 320°C
GC_EV01037
1
2 3
4
5 6
7
8
9
10
12 11
13
14
15
16
min.
NEW!
PAHs resolved in
less than10min.!
Website :
E-mail :
TelNo : 03 9762 2034 . . . inAUSTRALIA
Mar 2011
