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227

GC ACCESSORIES |

INSTRUMENT SUPPLIES

Connectors

Restek Press-Tight® Connectors

Obtaining a leak-tight seal:

To achieve optimum performance from these connectors, begin with a properly cut

fused silica column or retention gap end. Even if you use polyimide resin (cat.# 20445,

page 228)

for extra insurance, a poorly cut capillary column will make an inadequate

seal.

Press the cut ends into the connector, then establish a flow, and leak-check the seal with

a Restek® electronic leak detector (cat.# 22655,

page 220)

before heating the system.

What is the maximum temperature for a Press-Tight® connector?

Press-Tight® connectors are effective at oven temperatures up to 325 °C, the tem-

perature at which the polyimide coating on the column decomposes and the con-

nection will begin to leak. We strongly recommend using a Vu2 Union®

(page 229)

or SeCure® “Y”

(page 230

) connector if oven temperatures will exceed 325 °C for

prolonged periods of time.

Can Press-Tight® connectors be used with MXT® columns?

No. To achieve a leak-tight fused silica to stainless steel connection, we recommend an

MXT® connector (see

page 231

).

Make a clean, square cut for optimum

connector performance. The cut on the

right will produce a poor seal.

A brown ring indicates a proper seal.

Press-Tight® connectors are lightweight, quickly installed, and easy to use. They

connect fused silica tubing having outside diameters ranging from 0.33 to 0.74 mm

(Restek® 0.1 to 0.53 mm ID). Press-Tight® connectors do not cause solvent tailing, or

adsorb active compounds.

Press-Tight® connectors most often are used to connect a guard column to an ana-

lytical column. They also are used to connect columns differing in polarity, for unique

separations, or to repair a broken column.

*Additional cost will be added to the price of the column.

Let Restek Make the Connection!

Guard column connected

to an analytical column using

a Vu2 Union® connector.

Secure, reliable

column-to-column

connections!

Restek will connect a guard column/transfer line to any analytical

column, using a Vu2 Union® connector. We will leak-check the con-

nection and confirm analytical integrity by analyzing a test mixture.

To order a preconnected guard column/transfer line, add the three-

digit suffix from the chart below to any analytical column catalog

number. Example: A 5 m, 0.32 mm ID guard column connected to a

30 m, 0.32 mm ID, 1.0 µm Rtx®-5 column is cat.# 10254-163.

Guard columns

listed are

intermediate

polarity (IP)

deactivated.

For more

information

about guard

columns, see

pages 18–19

.

5m Guard Column ID cat.# suffix Additional Cost*

0.15 mm

-160

0.18 mm

-161

0.25 mm

-162

0.32 mm

-163

0.53 mm

-164

10m Guard Column ID cat.# suffix Additional Cost*

0.25 mm

-165

0.32 mm

-166

0.53 mm

-167

Our attention to detail is why Restek® products

are known for quality and reliability.