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113

GC COLUMNS |

METAL MXT® CAPILLARY COLUMNS

Application-Specific Columns: Petroleum & Petrochemical

Simulated Distillation Analysis (C5-C44)

Biodiesel Fuels Analysis

ASTM D6584 Derivatized B100 and Internal Standards on MXT®-Biodiesel TG

GC_PC00935

Column

MXT®-Biodiesel TG w/2 m x 0.53 mm retention

gap, 10 m, 0.32 mm ID, 0.10 µm (cat.# 70290)

Sample

B100 + IS butanetriol & tricaprin derivatized with

MSTFA as per ASTM D6584

Injection

Inj. Vol.:

1.0 µL cold on-column

Temp. Program:

Oven track

Oven

Oven Temp.:

50 °C (hold 1 min) to 180 °C at 15 °C/min to 230 °C

at 7 °C/min to 430 °C at 30 °C/min (hold 5 min)

Carrier Gas

H

2

, constant flow

Flow Rate:

4 mL/min

Detector

FID@ 430 °C

Note perfect solvent

peak shape!

free literature

Rtx®-2887/ MXT®-2887

Restek’s Capillary GC Columns

for Simulated Distillation of

Petroleum Fractions

Download your

free copy from

lit. cat.# 59567B

www.restek.com

free literature

Biodiesel Solutions:

Innovative Products

for Simple, Reliable

Biodiesel Analysis

Download your

free copy from

lit. cat.# PCFL1409-UNV

www.restek.com

MXT®-Biodiesel TG Columns

(Siltek®-treated stainless steel)

• Fast analysis times and sharp mono-, di-, and triglyceride peaks.

• Stable at 430 °C for reliable, consistent performance.

similar phases

MET-Biodiesel

*Total column length = 16 meters.

**Connected with low dead volume MXT connector.

MXT®-2887 Column

(Siltek®-treated stainless steel)

(nonpolar phase; Crossbond® 100% dimethyl polysiloxane—for simulated distillation)

• Application-specific columns for simulated distillation.

• Stable to 400 °C.

• 4.5

"

standard coil diameter.

MXT®-2887 columns’ stationary phase, column dimensions, and film thicknesses have

been optimized to exceed the resolution and skewing factor requirements specified in

ASTM Method D2887. Each column is individually tested to guarantee a stable base-

line with low bleed and reproducible retention times. The Crossbond® methyl silicone

stationary phase has increased stability compared to packed columns, ensuring stable

baselines and shorter conditioning times. Manufactured from Siltek®-treated stain-

less steel tubing, MXT® columns are the most durable high temperature GC columns

available.

similar phases

DB-PS2887

10-Meter

ID

df

temp. limits

cat.#

price

0.53 mm

2.65 µm

-60 to 360/400 °C

70199

3.5" Coil

7" diameter

11-pin cage

Description

temp. limits

cat.#

price

cat.#

price

14 m, 0.53 mm ID, 0.16 µm with 2 m Integra-Gap*

-60 to 380/430 °C 70289-273

70289

10 m, 0.32 mm ID, 0.10 µm

-60 to 380/430 °C

70292

10 m, 0.32 mm ID, 0.10 µm with 2 m x 0.53 mm Retention Gap** -60 to 380/430 °C

70290

15 m, 0.32 mm ID, 0.10 µm

-60 to 380/430 °C

70293

15 m, 0.32 mm ID, 0.10 µm with 2 m x 0.53 mm Retention Gap** -60 to 380/430 °C

70291

2 m x 0.53 mmMXT Biodiesel TG Retention Gap

-60 to 430 °C

70294