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www.restek.comGC COLUMNS |
GENERAL-PURPOSE COLUMNS
Stabilwax®
Six columns for the price of five!
Call 800-356-1688, ext. 3, or your Restek
representative for details!
FAMEs in Biodiesel Oils on Stabilwax®
GC_PC00916
Column
Stabilwax®, 30 m, 0.32 mm ID, 0.25 µm (cat.# 10624)
Sample
Tallow source of biodiesel (B100), prepared according
to European Method EN 14103
Injection
Inj. Vol.:
1.0 µL split (split ratio 100:1)
Liner:
Cyclosplitter® (cat.# 20706)
Inj. Temp.:
250 °C
Oven
Oven Temp.:
210 °C (hold 5 min) to 230 °C at 20 °C/min (hold 5 min)
Carrier Gas
H
2
, constant flow
Flow Rate:
3 mL/min
Linear Velocity:
60 cm/sec
Detector
FID@ 250 °C
Peaks
1. Myristic acid
C14:0
2. Palmitic acid
C16:0
3. Palmitoleic acid
C16:1
4. Stearic acid
C18:0
5. Oleic acid
C18:1
6. Linoleic acid
C18:2
7. Linolenic acid
C18:3
8. Arachidic acid
C20:0
9. Gadoleic acid
C20:1
10. Lignoceric acid
C24:0
11. Nervonic acid
C24:1
IS Methyl heptadecanoate
Tallow FAMEs in Biodiesel Oils on Stabilwax®
GC_PC00918
Peaks
1. Myristic acid
C14:0
2. Palmitic acid
C16:0
3. Palmitoleic acid
C16:1
4. Stearic acid
C18:0
5. Oleic acid
C18:1
6. Linoleic acid
C18:2
7. Linolenic acid
C18:3
8. Arachidic acid
C20:0
9. Gadoleic acid
C20:1
10. Behenic acid
C22:0
11. Erucic acid
C22:1
12. Lignoceric acid
C24:0
IS Methyl heptadecanoate
Yellow Grease FAMEs in Biodiesel Oils on Stabilwax®
Visit
www.restek.comfor soy FAMEs and
rapeseed FAMEs analyses.
also
available
Metal MXT® Columns
Rugged, flexible, Siltek®-treated stainless
steel tubing; inertness comparable to
fused silica tubing.
MXT®-WAX columns............
. page 110Stabilwax® Columns
(fused silica)
(polar phase; Crossbond® polyethylene glycol)
• Rugged enough to withstand repeated water injections.
• Low-bleed PEG column ensures long column lifetimes.
• Temperature range: 40 °C to 260 °C.
• Equivalent to USP G14, G15, G16, G20, and G39 phases.
Restek’s polar-deactivated surface tightly binds the Carbowax® polymer and increases
thermal stability, relative to competitive columns. Because of the increased stability
produced by the bonding process, Stabilwax® columns exhibit long column lifetimes,
even when programming repeatedly up to 260 °C. The bonding mechanism of the
column also produces polar compound retention times that do not shift, as is often
observed on other wax-type columns. In addition, this bonding mechanism produces
a column that can be rejuvenated by solvent washing. Stabilwax® columns are used for
a wide range of compounds and matrices including: FAMEs, flavor compounds, es-
sential oils, solvents, aromatics (including xylene isomers), acrolein/acrylonitrile (EPA
603), and oxygenated compounds. Also used for purity testing of chemicals and ana-
lyzing impurities in water matrices and alcoholic beverages.
Stabilwax® Structure
H
H
C C O
H
H
similar
phases
HP-INNOWax, CP-Wax 52 CB, VF-WAX MS,
ZB-WAXplus
*Maximum temperatures listed are for shorter length columns. Longer columns may have a different maximum temperature.
15-Meter
30-Meter
60-Meter
ID
df
temp. limits
cat.#
price
cat.#
price
cat.#
price
0.25 mm 0.10 µm 40 to 250/260 °C 10605
10608
10611
0.25 µm 40 to 250/260 °C 10620
10623
10626
0.50 µm 40 to 250/260 °C 10635
10638
10641
0.32 mm 0.25 µm 40 to 250/260 °C 10621
10624
10627
0.50 µm 40 to 250/260 °C 10636
10639
10642
1.00 µm 40 to 240/250 °C 10651
10654
10657
0.53 mm 0.25 µm 40 to 250/260 °C 10622
10625
10628
0.50 µm 40 to 250/260 °C 10637
10640
10643
1.00 µm 40 to 240/250 °C 10652
10655
10658
1.50 µm 40 to 230/240 °C 10666
10669
10672
2.00 µm 40 to 220/230 °C 10667
10670
10-Meter
20-Meter
ID
df
temp. limits
cat.#
price
cat.#
price
0.15 mm 0.15 µm 40 to 250/260 °C 43830
43831
0.18 mm 0.18 µm 40 to 250 °C
40602