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REFERENCE STANDARDS |
ENVIRONMENTAL
Pesticides
Pesticides, Chlorinated/Organochlorine/Organohalide,
cont.
04.2, 04.1, 03.2, 3/90, 4/89, and 2/88 SOW (Pesticides), QA Mixes
Pesticide Surrogate Mix
(2 components)
See cat.#s 32000 and 32457 on
page 524.
1,000 µg/mL in acetone, 1 mL/ampul
cat.# 32017 (ea.)
2,4,5-Trichlorophenol (95-95-4)
Florisil® Cartridge Check Standard
(2,4,5-Trichlorophenol)
In methyl
tert
-butyl ether, 1 mL/ampul
cat.# 32417 (ea.)
4,4'-DDT (50-29-3)
200 µg/mL
Endrin (72-20-8)
100 µg/mL
Organochlorine Pesticide System Evaluation Mix
(2 components)
• Designed for daily assessment of system performance.
• Reveals active sites in the injection port and/or GC column.
• Prepared in MTBE—low expansion volume helps minimize
backflash.
In hexane, 1 mL/ampul
cat.# 32002 (ea.)
α
-BHC (319-84-6)
1 µg/mL
β
-BHC (319-85-7)
1
γ
-BHC (Lindane) (58-89-9)
1
4,4'-DDT (50-29-3)
10
Endrin (72-20-8)
5
Methoxychlor (72-43-5)
25
Pesticide Performance Evaluation Mix
(6 components)
In hexane, 1 mL/ampul
cat.# 32074 (ea.)
α
-BHC (319-84-6)
1 µg/mL
β
-BHC (319-85-7)
1
γ
-BHC (Lindane) (58-89-9)
1
4,4'-DDT (50-29-3)
10
Decachlorobiphenyl (SS) (2051-24-3) 2
Endrin (72-20-8)
5
Methoxychlor (72-43-5)
25
2,4,5,6-Tetrachloro-
m
-xylene (SS)
(877-09-8)
2
Pesticide Performance Evaluation Mix w/Surrogates
(8 components)
Working with solutions containing decachlorobiphenyl
Decachlorobiphenyl has poor solubility in most organic solvents.
The maximum concentration that can be prepared in acetone,
hexane, or isooctane is 200 µg/mL. Temperature will affect the solu-
bility as well. Storing solutions at reduced temperatures will cause
decachlorobiphenyl to precipitate.
Products containing decachlorobiphenyl must be sonicated for a
minimum of 10 minutes prior to opening the ampul. Because each
ultrasonic bath operates at a different energy level, 10 minutes is
a guideline only. Longer sonication time will not affect product
quality.
These precautions apply to working solutions prepared in your
laboratory as well. The amount of compound that precipitates
depends on concentration AND temperature. If you store your
standards at a temperature lower than 4 °C (even dilute solutions),
allow extra sonication time.
tech tip
also available
200+ compound
multiresidue pesticides
standard kits for LC-MS/MS
and GC-MS/MS!
See
pages 568–571 .200 µg/mL in acetone, 1 mL/ampul
cat.# 32027 (ea.)
200 µg/mL in acetone, 5 mL/ampul
cat.# 32028 (ea.)
2,4,5,6-Tetrachloro-
m
-xylene (877-09-8)
2,4,5,6-Tetrachloro-
m
-xylene
200 µg/mL in acetone, 1 mL/ampul
cat.# 32029 (ea.)
200 µg/mL in acetone, 5 mL/ampul
cat.# 32030 (ea.)
10 µg/mL in isooctane, 1 mL/ampul
cat.# 32289 (ea.)
Decachlorobiphenyl (BZ #209) (2051-24-3)
Decachlorobiphenyl (BZ #209)
200 µg/mL in acetone, 1 mL/ampul
cat.# 32025 (ea.)
Dibutylchlorendate (1770-80-5)
Dibutylchlorendate
CLP Pesticides Mixtures, QA Mixes
In acetone, 1 mL/ampul
cat.# 32018 (ea.)
Aldrin (309-00-2)
25 µg/mL
γ
-BHC (Lindane) (58-89-9)
25
4,4'-DDT (50-29-3)
50
Dieldrin (60-57-1)
50
Endrin (72-20-8)
50
Heptachlor (76-44-8)
25
Pesticide Matrix Spike Mix
(6 components)
For complete listing of PCB reference standards, see pages
530–531.Low-Concentration Pesticides Mixtures,
QA Mixes
In acetone, 1 mL/ampul
cat.# 32040 (ea.)
γ
-BHC (Lindane) (58-89-9)
10 µg/mL
trans
-Chlordane (5103-74-2)
10
4,4'-DDE (72-55-9)
20
Dieldrin (60-57-1)
20
Endosulfan sulfate (1031-07-8)
20
Endrin (72-20-8)
20
Heptachlor epoxide (isomer B)
(1024-57-3)
10
L/C Pesticide Lab Control Sample
(7 components)