472
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Acylation Derivatization Reagents
• Most commonly used for electron capture detection.
• React with alcohols, amines, and phenols.
• Frequently used for drugs of abuse confirmation.
Acylation reagents offer the same advantage available from si-
lylation reagents: creating less polar, more volatile derivatives.
In comparison to silylating reagents, the acylating reagents can
more readily target highly polar multifunctional compounds,
such as carbohydrates and amino acids. In addition, acylating
reagents offer the distinct advantage of introducing electron-
capturing groups, thus enhancing detectability during analysis.
Compound
CAS #
cat.#
price
MBTFA (N-methyl-bis-trifluoroacetamide)
10-pk. (10x1 g)
685-27-8
35616
25 g vial
685-27-8
35617
TFAA (trifluoroacetic acid anhydride)
10-pk. (10x1 g)
407-25-0
35618
25 g vial
407-25-0
35619
PFAA (pentafluoropropionic acid anhydride)
10-pk. (10x1 g)
356-42-3
35620
25 g vial
356-42-3
35621
HFAA (heptafluorobutyric acid anhydride)
10-pk. (10x1 g)
336-59-4
35622
25 g vial
336-59-4
35623
PFPOH (pentafluoropropanol)
10-pk. (10x1 g)
422-05-9
35624
25 g vial
422-05-9
35625
Deactivating Agent
Derivatization Reagents
Reference
Standards
Column & Detector
Test Mixes & Reagents
Deactivating Agent..........................................
472Derivatization Reagents.......................
472–473Detector Tuning Mixtures.............................
473GC Column & Detector Test Mixes..
473–474GPC Calibration Mixes.....................................
474LC Column & Detector Test Mixes.............
475Neat, 25 mL/bottle
cat.# 31861 (ea.)
Ground transportation shipments only.
No data pack available.
Dimethyldichlorosilane (DMDCS) (75-78-5)
Dimethyldichlorosilane (DMDCS) Deactivating Agent
• Easy deactivation of liners and other glass surfaces.
• Convenient—25 mL bottle deactivates 60 inlet liners.
• Tested to ensure consistent quality and effectiveness.
Restek offers dimethyldichlorosilane (DMDCS) for deactivating
liners and other glassware. DMDCS reacts with active hydroxyl
groups on the glass surface to produce a deactivated surface. A
simple, step-by-step procedure is included with the product.
— Buy 3 Standards, Get 10% Off
— Buy 5 Standards, Get 20% Off
Quantity Discounts Available
Not available for all standards. Contact your local
Restek® representative for more details.