100 www.restek.com
Rapid analysis of volatile organics in US EPA Method 8260B, on an Rtx
®
-VMS column.
min.
2
4
6
8
10
2
1
3
4
5
6
7
8
9 10
11
13
14
15
16
17
18
19-21
22
23
24
25
26-28
29-32
33,34
35
36 37
38
39
40
41
42
43
44
45
46 47
48
49
50
51
52
53
54,55
56
57
58
59
60
61
62,
63
64,65
66,67
68,69
70
71,72
73
74
75
76
77
78
79,80
81
82,83
84
85
86
87
88,89
90
91
92
93
94
95
96
97
GC_EV00428
12
Column:
Rtx
®
-VMS, 20m, 0.18mm ID, 1.00µm (cat.# 49914)
Conc.:
10ppb in 5mL of RO water
unless otherwise noted; ketones at 2.5X
Concentrator:
Tekmar LSC-3100 Purge and Trap
Trap:
Vocarb 3000 (type K)
Purge:
11 min. @ 40mL/min. (ambient temperature)
Dry purge:
1 min. @ 40mL/min.
Desorb preheat: 245°C
Desorb:
250°C for 2 min., flow 40mL/min.
Bake:
260°C for 8 min.
Interface:
0.53mm ID Silcosteel
®
tubing transfer line
1:40 split at injection port. 1mm ID liner.
Oven temp.:
50°C (hold 4 min.) to 100°C @ 18°C/min. (hold 0 min.)
to 230°C @ 40°C/min. (hold 3 min.)
Carrier gas:
helium @ ~1.0mL/min. constant flow
Adjust dichlorodifluoromethane to a retention time of 1.03 min. @ 50°C.
Detector:
Agilent 5973 MSD
Scan range:
35-300amu
For peak listing, see page 550.
Rtx®-VMS Columns
(fused silica)
(proprietary Crossbond® phase)
• Application-specific columns for volatile organic pollutants by GC/MS.
• Complete separation of US EPA Method 8260B compounds in less than 10 minutes.
• Stable to 260 °C.
• No known equivalent phases.
Rtx®-VMS columns offer lower bleed, better selectivity, and overall faster analysis fo
separating volatile organic compounds, such as those listed in US EPA Method 8260B
The Rtx®-VMS stationary phase is a highly stable polymer that provides outstandin
analysis of volatile compounds, in combination with sensitive ion traps and Agilen
5973 mass spectrometers. 0.18 and 0.25 mm ID columns allow sample splitting at th
injection port, eliminating the added expense and maintenance of a jet separator. A 0.4
mm or 0.53 mm ID column can be directly connected to the purge & trap transfer lin
in a system equipped with a jet separator.
ID
df
temp. limits
30-Meter
60-Meter
75-Meter
0.25mm 1.40µm -40 to 240/260°C 19915
19916
0.32mm 1.80µm -40 to 240/260°C 19919
19920
0.45mm 2.55µm -40 to 240/260°C 19908
19909
0.53mm 3.00µm -40 to 240/260°C 19985
19988
19974
ID
df
temp. limits
20-Meter
40-Meter
0.18mm 1.00µm -40 to 240/260°C 49914
$450
49915
$755
Website : www.chromtech.net.au E-mail : info@chromtech.net.au TelNo : 03 9762 2034 . . . in AUSTRALIA Mar