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GC COLUMNS |
APPLICATION-SPECIFIC COLUMNS
Petroleum & Petrochemical
Biodiesel Fuels Analysis
Integra-Gap®
technology
• Built-in retention gap.
• Eliminates connector and leaks.
• Extends analytical column lifetime.
Retention Gap
Liquid Phase
free
literature
Biodiesel Solutions:
Innovative Products
for Simple, Reliable
Biodiesel Analysis
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lit. cat.# 580207
Derivatized B100 and internal standards on an MXT®-Biodiesel TG column with 2 m x 0.53 mm ID coupled
retention gap, according to ASTM D6584.
GC_PC00935
monoglycerides
triglycerides
Column:
MXT
®
-Biodiesel TG, 10m, 0.32mm ID, 0.1µm
with 2m x 0.53mm retention gap (cat.# 70290)
Sample:
B100 + IS butanetriol & tricaprin derivatized
with MSTFA as per ASTM D-6584
Inj.:
1.0µL cool on-column
Inj. temp.:
oven track
Carrier gas:
hydrogen, constant flow
Flow rate:
4mL/min.
Oven temp.:
50°C (hold 1 min.) to 180°C @ 15°C/min.,
to 230°C @ 7°C/min., to 430°C @ 30°C/min.
(hold 5 min.)
Det.:
FID @ 430°C
butanetriol (IS)
glycerin
tricaprin (IS)
diglycerides
Note perfect peak
shape of solvent, with
low-dead-volume
MXT® connector.
Rtx®-Biodiesel TG Columns
(fused silica)
• Linearity for all reference compounds exceeds method requirements.
• Alumaseal® connector provides leak-free connection; guard column
extends column life.
• Low column bleed at high temperatures.
• For glycerine and glycerides analysis, according to ASTM D6584 and
EN 14105 methods.
*Total column length = 16 meters.
**Connected with low-dead-volume MXT connector.
MXT®-Biodiesel TG Columns
(Siltek® treated stainless steel)
• Fast analysis times and sharp mono-, di-, and triglyceride peaks.
• Stable at 430 °C for reliable, consistent performance.
• Integra-Gap® built-in retention gap on 0.53 mm ID column eliminates
column coupling completely.
Description
temp. limits
cat.#
price
10m, 0.32mm ID, 0.10µm
to 330/380°C 10292
10m, 0.32mm ID, 0.10µm with 2m x 0.53mm ID Retention Gap
to 330/380°C 10291
15m, 0.32mm ID, 0.10µm
to 330/380°C 10294
15m, 0.32mm ID, 0.10µm with 2m x 0.53mm ID Retention Gap
to 330/380°C 10293
Description
temp. limits
cat.#
price
14m, 0.53mm ID, 0.16µm with 2m Integra-Gap*
-60 to 380/430°C 70289
10m, 0.32mm ID, 0.10µm
-60 to 380/430°C 70292
10m, 0.32mm ID, 0.10µm with 2m x 0.53mm Retention Gap**
-60 to 380/430°C 70290
15m, 0.32mm ID, 0.10µm
-60 to 380/430°C 70293
15m, 0.32mm ID, 0.10µm with 2m x 0.53mm Retention Gap**
-60 to 380/430°C 70291
2m x 0.53mm MXT Biodiesel TG
70294
Website : www.chromtech.net.au E-mail : info@chromtech.net.au TelNo : 03 9762 2034 . . . in AUSTRALIA
Mar 2011