GC-TOFMSConditions
GasChromatography
Onemicroliter splitless 250°C, 60 sec valve
60m x 0.18mm x 0.18µmRestekRtx-PCBcolumn
Constant flow helium, 1.5mL/minute
70°C (1min), 50°/min to 120°, 3°/min to360° (1min)
MassSpectrometry LECOPegasus III
Source temperature: 225°C
Electron ionization: 70 eV
Storedmass range: 120 to520u
Acquisition rate: 5 spectra/sec
