GCConditions
Split injection
– 4mmRestekSiltek linerwithSiltekwool
– Onemicroliter at 250°C
– Split ratio 50:1
– 10mx 0.18mmx 0.18µmRestekRtx-5SilMS column
– Constant flow helium, 2mL/minute
GCovenprogram
– 40°C (0.1min), 30°/min to 340°(0 min)
– 25 sec solvent delay
– Total run time: 10min
