Residual Solvents: RunConditions
Dual FIDs@ 250°C
Dual FIDs@ 250°C
Detectors
0.2
µ
LHS, 200:1 split
0.2
µ
LHS, 200:1 split
Injection
230°C
230°C
Injector
2.5mL/min. to 9.5min.
3.5mL/min. at 10min.
1.5mL/min.
constant flow
ColumnFlow
40°C (1min. hold)
to 65°C at 6°C/min.,
to 100°C at 12°C/min.,
to 250°C at 70°C/min.,
1.8min. hold
40°C (6min. hold)
to 100°C at 4°C/min.,
to 220°C at 15°C/min.,
5min. hold
OvenProgram
Stabilwax
15m x 0.25mm, 0.5
µ
m
Rtx-200
30m x 0.25mm, 1
µ
m
Stabilwax
15m x 0.25mm, 0.5
µ
m
Rtx-200
30m x 0.25mm, 1
µ
m
Analytical
Columns
Fast Procedure
StandardProcedure
