AnalysisConditions
30m, 0.25mmID, 0.50µmRtx-5MS (cat.#12638)
2µL splitless injection. On-column concentration: 20ng.
Oven temp.:
40°C(hold2min.) to 300°C@
10°C/min. (hold4min.), to330°C
@10°C/min. (hold 10min.).
Inj. / det. temp.:
280°C / 300°C
Det. type:
MS
Carrier gas:
helium
Linear velocity:
32 cm/sec. set
@40°C
Ionization:
EI
Splitless hold:
0.5min.
ScanRange:
35-500AMU
