Experimental Conditions
•
Rtx
R
®
-5SilMS
–
30mx0.25mm ID, 0.25um film
•
Drilled
r
Uniliner
®
–
Eliminatemetal contact in injectionport
•
Standard concentration
–
4, 10, 16, 24, 32, 80 ng/µl
–
ISTD at 8ng/µl
•
1µl injections, 0.4min. purge time
•
Injectionport temp. at 300°C
•
HP6890w/5973GC/MS
•
35°C (2min.) 20°C/min. 260° (0min.)
6°C/min. 330° (1min.)
