585
GC CHROMATOGRAMS |
ENVIRONMENTAL
PCB Mixtures
GC_EV00992A
GC_EV00994A
GC_EV00993A
GC_EV00997A
GC_EV00996A
GC_EV00995A
Aroclor 1221
Aroclor 1232
Aroclor 1016
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Rtx®-CLPesticides2
30m, 0.32mm ID, 0.25μm (cat.# 11324)
1
1
1
1
1
1
1
1. decachlorobiphenyl (DCB)
Column:
Rtx
®
-CLPesticides2, 30m, 0.32mm ID, 0.25µm (cat.# 11324)
Sample:
1,000µg/mL each Aroclor compound in hexane diluted to 1,000ppb,
decachlorobiphenyl (BZ #209) 200µg/mL in acetone (cat.# 32029)
diluted to 100ppb
Inj.:
1.0µL pulsed splitless @ 30psi (hold 0.3 min.),
4mm cyclo double gooseneck inlet liner (cat.# 20895)
Inj. temp.:
250°C
Carrier gas:
helium, constant flow
Linear velocity: 60cm/sec. @ 120°C
Oven temp.:
120°C to 200°C @ 45°C/min. to 230°C @ 15°C/min.
to 330°C (hold 2 min.) @ 30°C/min.
Det.:
µ-ECD @ 330°C
Aroclor PCBs
US EPA Method 8082
Rtx®-CLPesticides2
GC_EV00998A
Website :
E-mail :
TelNo : 03 9762 2034 . . . in AUSTRALIA
Mar 2011
