Fittings-Chromatography-2014 - page 464

Holes for 1/8”
OD tubing
Additional hole
for luer
Holes for 1/8”
OD tubing
Additional hole
for luer
20µm
stainless
steel frit
BottleCapPlugs&Adapters
Use theA-626BottleCapPlug to seal the third “tapered” luer hole
found inmost Upchurch Scientific
®
BottleCaps. Or, use theA-628
Plug to seal anyunused1/16”or 1/8”bottlecapholes.
Alternatively, try theA-627or A-629Filter BottleCapPlug to cap an
unusedhole in your bottle cap. The20µm stainless steel frit in these
products prevents foreignmatter from contaminating your solvent
while leaving thebottleopen to theatmosphere, thus allowingfluid
tobepulledoutwithout creatinga vacuum (generally not usedwith
spargingapplications). All plugbodies aremanufactured fromultra-
highmolecularweight polyethylene (UHMWPE).
A-626
BottleCapPlug
A-629
Filter BottleCapPlug
BottleCaps
XX
Extremely simple—no threadedports or fittings
XX
Manufactured fromETFE andPolypropylene
If you are looking for abottle cap that is quick andeasy touse, but
still allowsmany connection options, we have just what you need!
TheBottleCaps fit standardGL-45 (1 L) or smaller-neckGL-38 (4 L)
glassbottles.
Eachcaphas threeholes.With twoof theholesyou simplypushyour
tubing straight through. The thirdhole,witha luer taper, canbeused
foranumberofoptions.Anymale luer (suchasa luer-locksyringe)willfit
snugly in thishole,oryoucanuse theA-626orA-627Plug.Exceptions
are theA-610andA-610BBottleCaps. Please see thenotebelow.
A-622
GL-38BottleCap
for 1/8” tubing
A-620
GL-45BottleCap
for 1/8” tubing
APPLICATIONNOTE
XX
A self-regulating sparging systemcanhelp reducehelium
consumptionand improvepumpperformance. Set thisupby
pressing your tubing through theappropriateholes in your bottle
capandattachingeach line toafilter. Sparge yourmobilephase
withan inert gas (preferablyhelium) for 15–20minutes. Then
reduce theoutlet pressureof the sparginggas toamaximumof 5
psi (0.34bar) and insert aplug (A-626orA-628) into the remaining
port of thecap. The sparginggaswill shut off once the incoming
pressureequals thepressure inside the reservoir. As themobile
phase is consumedand the internal pressure lowers, sparginggas
will enter tokeep the systempressurizedanddegassed. Please
Note: If gas leakswhilepressurizing thebottle, try removing the
sealing ring from thebottle, as it sometimes interfereswith the
sealingof thesebottlecaps.
XX
One concernwith sparging systems is thepossibilityof solvent
backingup the sparging inlet line. This canoccur if thegas tank
completely evacuateswith the regulating valves open, creating
a vacuum in the tubing. Solvent backupmaydamage sparging
system components and cause cross-contaminationofmobile
phase reservoirs. Tohelpprevent solvent backup, install the
CV-3010 InlineCheckValve (page 151) along the tubing line that
runs between thegas supply and the solvent bottle.
XX
For amoreefficient degassing system, please see theSystec
®
HPLCVacuumDegassingSystems onpage 178.
XX
Please see theQuick-Stop Luer CheckValveonpage 151
for another solvent inlet ApplicationNote.
NOTE
TheA-610andA-610BBottleCapshaveaslightlydifferentconfiguration
than theothercaps.Oneholeaccepts3/16”OD tubing, the typical size
usedwithsomeWaters
®
systems.The remaining twoholesaccept1/8”OD
tubing.Unlike theothercaps, theA-610doesnothavea tapered luerhole.
Ifdesired,useourA-628PlugorA-629FilterPlug foroneof the1/8”holes.
RELATEDPRODUCTS
Toensurea tight seal, useUpchurchScientificfluoropolymer tubingwith
thesebottlecaps (pages70–73).
PartNo.
Description
BOTTLECAPSFORGL-45, 1 LBOTTLES
A-610
for 3/16”OD tubing, Red
A-610B
for 3/16”OD tubing,Blue
A-620
for 1/8”OD tubing, Red
A-620B
for 1/8”OD tubing,Blue
A-630
for 1/16”OD tubing, Red
A-630B
for 1/16”OD tubing,Blue
BOTTLECAPSFORGL-38, 4 LBOTTLES
A-622
for 1/8”OD tubing,Black
BOTTLECAPPLUGSANDADAPTER
A-626
BottleCapPlug for luerhole,UHMWPE
A-627
FilterBottleCapPlug for luerhole,UHMWPE
with20µm stainless steel frit
A-628
BottleCapPlug for 1/16”, 1/8”or 3/16”hole,UHMWPE
A-629
FilterBottleCapPlug for 1/16”, 1/8”or 3/16”hole,UHMWPE
with20µm stainless steel frit
FILTERS&COLUMNACCESSORIES
159
BottleCaps&Plugs
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