USP 467
Residual Solvents (OVIs) Headspace
1.MethyleneChloride
2.Chloroform
3. Benzene
4. 1,1,1 - trichloroethylene
5. 1,4 - dioxane
Analysis carried out withDANI Master GC.
Column:
MEGA-624 FAST - 0.10mm,0.45µm,10m
Catalog Code: F-624-010-045-10
Conditions:
Injection: Split 250°C, 0.5mLwithGas Syringe, 1:100 Split Ratio.
Sample:Headspace of Residual SolventsMix, hold 45min@
80°C.
Detector: FID 250°C.
Oven Program: 35°C, 15°C/min, 100°C.
Carrier Gas:Hydrogen, 0.4mL/min.
MEGA s.n.c - Capillary Columns Laboratory -Via Plinio, 29 - 20025 Legnano (MI) - Italy - tel./fax:+39 0331.54.79.24 -
-
Since 1980
3min
1
2
3
4
5
(USPG43 phase)
