Testing Protocol for Amines
Column: 30m, 0.32mm ID, I.Oum Rtx.-35 Amine
Standard
Mix:
Amine test mix
in
50:50 CH
2CI:/MeOH
Injection volume: IJlI, 7673 autosampler
Injection type: splitless
Hold
time:
lmin
Injector temperature: 250°C
Carrier
gas:
helium (9psi
head
pressure, constant pressure)
Oven
temperature:
40·C (Imin)
to
16S·C (Imin)@1O"C1min,
to
280·C(10min)
@W·C/min
GC:
Agilent
5890
Detector
I
Temperature: FID
I
310°C
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