585
GCCHROMATOGRAMS |
ENVIRONMENTAL
PCB Mixtures
GC_EV00992A
GC_EV00994A
GC_EV00993A
GC_EV00997A
GC_EV00996A
GC_EV00995A
Aroclor 1221
Aroclor 1232
Aroclor 1016
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Rtx®-CLPesticides2
30m, 0.32mm ID, 0.25μm (cat.#11324)
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1
1
1
1
1
1
1. decachlorobiphenyl (DCB)
Column:
Rtx
®
-CLPesticides2, 30m, 0.32mm ID, 0.25µm (cat.# 11324)
Sample:
1,000µg/mL each Aroclor compound in hexane diluted to 1,000ppb,
decachlorobiphenyl (BZ#209) 200µg/mL in acetone (cat.# 32029)
diluted to 100ppb
Inj.:
1.0µL pulsed splitless@ 30psi (hold 0.3min.),
4mm cyclo double gooseneck inlet liner (cat.# 20895)
Inj. temp.:
250°C
Carrier gas:
helium, constant flow
Linear velocity: 60cm/sec.@ 120°C
Oven temp.:
120°C to 200°C@ 45°C/min. to 230°C@ 15°C/min.
to 330°C (hold 2min.)@ 30°C/min.
Det.:
µ-ECD@ 330°C
AroclorPCBs
USEPAMethod8082
Rtx®-CLPesticides2
GC_EV00998A
Website :
E-mail :
TelNo : 03 9762 2034 . . . inAUSTRALIA
Mar 2011
