641
GCCHROMATOGRAMS |
FOODS, FLAVORS&FRAGRANCES
Fragrances
GC_FF00657
5%FragranceMaterialsAssociationMix
Rtx®-1
Column:
Rtx
®
-1, 60m, 0.25mm ID, 0.25µm
(cat.# 10126)
Sample:
5% FMAmix in acetone (cat.# 31807)
Inj.:
1.0µL split (split ratio 40:1),
4mm inlet liner (cat.# 20814)
Inj. temp.:
285°C
Carrier gas:
helium, constant flow
Flow rate:
0.6mL/min.
Oven temp.:
50°C to 270°C@ 3°C/min.
Det.:
FID@ 300°C
Compound
% in the FMAmix
1. ethyl butyrate
35.7
2. limonene
20.0
3. eucalyptol
0.5
4. benzoic acid
1.0
5. cinnamic aldehyde
0.5
6. geraniol
0.6
7. hydroxycitronellal
5.0
8. thymol
0.3
9. cinnamyl alcohol
0.3
10. vanillin
0.1
11. cinnamyl acetate
0.3
12. benzyl salicylate
35.7
FMAReferenceMix
cat.#31807
5%FragranceMaterialsAssociationMix
Rtx®-1701
GC_FF00658
Column:
Rtx
®
-1701, 60m, 0.25mm ID, 0.25µm (cat.# 12026)
Sample:
5% FMAmix in acetone
Inj.:
1.0µL split (split ratio 40:1), 4mm inlet liner (cat.# 20814)
Inj. temp.:
285°C
Carrier gas:
helium, constant flow
Flow rate:
0.6mL/min.
Oven temp.:
50°C to 270°C@ 3°C/min.
Det.:
FID@ 300°C
Compound
% in FMAMix
1. ethyl butyrate
35.7
2. limonene
20.0
3. eucalyptol
0.5
4. geraniol
0.6
5. benzoic acid
1.0
6. cinnamic aldehyde
0.5
7. hydroxycitronellal
5.0
8. thymol
0.3
9. cinnamyl alcohol
0.3
10. cinnamyl acetate
0.3
11. vanillin
0.1
12. benzyl salicylate
35.7
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E-mail :
TelNo : 03 9762 2034 . . . inAUSTRALIA
Mar 2011
