ORGANOCHLORINATEDPESTICIDES–EPAMETHOD608/8081
MEGA-5
I.D.
0.32mm
T start
65°C
25m
Rate1
T2
150°C
Rate2
Tend
260°C
Detector
FID
280°C
1
2
3
4
5
6
7
8
9
4,4' DDE
10
11
12
4,4' DDD
13
14
15
4,4' DDT
16
Column
ChroamtographicConditions
Phase
Injection
On column
Injection volume
1.0 µL
FilmThickness
0.25 µm
Oven
Length
20°C/min
7°C/min
CarrierGas
Hydrogen 60 kPa
Peak Identification
α-BHC
β-BHC
γ-BHC
δ-BHC
Heptachlor
Aldrin
Heptachlor epoxide
Endosulfan I
Dieldrin
Endrin
Endosulfan II
Endrinaaldehyde
Endosulfan sulfate
