MEGA-BIODIESEL105
PTV
50°CT1
1
I.D.
0.32mm
RatePTV
2 Internal Standard 1
T2PTV 360°C (15min)
3
15m
T 1
50°C (1min)
4 Internal Standard 2
Rate
5
T2
180°C
6
Rate 2
T3
230°C
Rate 3
10°C
T4
370°C (5min)
BIODIESEL –Determinationof Free andTotal Glycerol andmono-, di-, tryglicerides (According toUNI EN ISO 14105 andASTM6584)
Column
GCConditions
Identification
StationaryPhase
Injector
Glycerol
999°C/min
FilmThickness
0.1 µm
Monoolein
Length
Oven
15°C/min
Diolein
Sample
Triolein
Standardmixtureof Glycerol andmono-, di-,
7°C/min
triglycerides derivatizedwithMSTFA
CarrierGas
Helium 3mL/min
Results carriedoutwithDANI GCMASTER
